Title |
Facile synthesis of silver-doped zinc oxide nanostructures as efficient scaffolds for detection of p-nitrophenol / |
Authors |
Thakur, Deepika ; Sharma, Anshu ; Singh Rana, Dharmender ; Thakur, Nagesh ; Singh, Dilbag ; Tamulevicius, Tomas ; Andrulevicius, Mindaugas ; Tamulevicius, Sigitas ; Shukla, Sudheesh K ; Thakur, Sourbh |
DOI |
10.3390/chemosensors8040108 |
Full Text |
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Is Part of |
Chemosensors.. Basel : MDPI. 2020, vol. 8, iss. 4, art. no. 108, p. 1-15.. ISSN 2227-9040 |
Keywords [eng] |
Ag-doped ZnO ; solution combustion ; luminescence ; p-nitrophenol sensing |
Abstract [eng] |
In this paper, silver-doped zinc oxide nanoparticles were synthesized by using a solution combustion technique, in which zinc nitrate is used as an oxidizer and tartaric acid as a fuel. The phase composition, morphology and structural properties of the as-synthesized zinc oxide and silver-doped zinc oxide were established by using powdered X-ray diffraction, field emission scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy studies. Due to well-defined morphologies and crystallinity, the pure zinc oxide and silver-doped zinc oxide nanostructures can be used as effcient chemical sensors for the detection of p-nitrophenol (PNP). ZnO was found to show a low value of the limit of detection (LOD), i.e., 2.175 μM/L, for p-nitrophenol sensing; moreover, a sharp decrease in the limit of detection was observed with an increase in the concentration of silver ions, and the LOD value decreased to 0.669 μM/L for 10 mol % silver-doped zinc oxide. It is therefore concluded that Ag-doped ZnO shows a lower limit of detection as compared to pure ZnO for p-nitrophenol sensing. |
Published |
Basel : MDPI |
Type |
Journal article |
Language |
English |
Publication date |
2020 |
CC license |
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